Stereochemistry

R/S configuration, chirality, and 3D molecular structure

Cahn-Ingold-Prelog Priority Rules

1

Higher Atomic Number = Higher Priority

Look at atoms directly attached to chiral center

Priority: I (53) > Br (35) > Cl (17) > S (16) > F (9) > O (8) > N (7) > C (6) > H (1)

2

If Tied, Go to Next Atom

Move outward from chiral center atom by atom

Example: -CH₂CH₃ vs -CH₃ → Both start with C, but ethyl has another C while methyl has H

3

Multiple Bonds Count as Multiple Atoms

C=O treated as C bonded to two O's

• C=O → C bonded to (O, O, _)

• C≡N → C bonded to (N, N, N)

• C=C → each C bonded to (C, C, _)

4

Assigning R/S Configuration

Step-by-Step Procedure

1.

Identify the chiral center

Carbon with four different groups attached

2.

Assign priorities (1-4)

Using Cahn-Ingold-Prelog rules, 1 = highest, 4 = lowest

3.

Orient molecule

Put lowest priority (#4) in the back (away from you)

4.

Trace 1 → 2 → 3

If clockwise = R (Rectus, right)
If counterclockwise = S (Sinister, left)

Memory Aid

R = Right turn (clockwise) 🔄

S = Sinister (left/counterclockwise) 🔃

Worked Example

Example: 2-Bromobutane

Structure:

CH₃-CHBr-CH₂-CH₃

Step 1: Identify chiral center

C2 (the carbon with Br attached) has 4 different groups:

  • • Br
  • • H
  • • CH₃ (to the left)
  • • CH₂CH₃ (to the right)

Step 2: Assign priorities

1BrHighest atomic number (35)
2-CH₂CH₃C attached to (C, H, H) vs methyl's (H, H, H)
3-CH₃C attached to (H, H, H)
4HLowest priority

Step 3: Orient (H to the back)

Imagine looking at the molecule with H pointing away from you

Step 4: Trace 1 → 2 → 3

Br (1) → CH₂CH₃ (2) → CH₃ (3)

If clockwise: (R)-2-bromobutane

If counterclockwise: (S)-2-bromobutane

(Actual configuration depends on 3D orientation - both enantiomers exist!)

Types of Stereoisomers

Enantiomers

Definition: Non-superimposable mirror images

Properties:

  • • Opposite R/S configurations at all chiral centers
  • • Identical physical properties (mp, bp, density)
  • • Rotate plane-polarized light in opposite directions
  • • Different biological activity (one may be drug, other inactive/toxic)

Example: (R)-ibuprofen vs (S)-ibuprofen

Diastereomers

Definition: Stereoisomers that are NOT mirror images

Properties:

  • • At least one (but not all) chiral center has opposite configuration
  • • Different physical properties (mp, bp, solubility)
  • • Different chemical reactivity
  • • Can be separated by standard techniques (crystallization, chromatography)

Example: (2R,3R)-tartaric acid vs (2R,3S)-tartaric acid

Meso Compounds

Definition: Achiral molecule with chiral centers (internal plane of symmetry)

Properties:

  • • Contains 2+ chiral centers but overall achiral
  • • Internal mirror plane cancels optical activity
  • • Does NOT rotate plane-polarized light

Example: (2R,3S)-tartaric acid = meso-tartaric acid

Number of Stereoisomers

Maximum stereoisomers = 2ⁿ

where n = number of chiral centers

Examples:

  • • 1 chiral center → 2¹ = 2 stereoisomers (1 pair of enantiomers)
  • • 2 chiral centers → 2² = 4 stereoisomers (2 pairs of enantiomers, unless meso)
  • • 3 chiral centers → 2³ = 8 stereoisomers

Exception: Meso compounds reduce the count!

If molecule has internal symmetry, actual # < 2ⁿ

Optical Activity

Specific Rotation [α]

[α] = α / (l × c)

α = observed rotation (degrees)

l = path length (dm)

c = concentration (g/mL)

Terminology

(+) or d = dextrorotatory (rotates right)

(-) or l = levorotatory (rotates left)

Important: (+)/(-) ≠ R/S!
R can be (+) or (-), determined experimentally

Common Mistakes

⚠️

Forgetting to Put #4 in Back

If #4 is in front, your R/S assignment will be backwards!

⚠️

Confusing R/S with (+)/(-)

R/S is configuration (structure). (+)/(-) is optical rotation (experimental).

⚠️

Missing Chiral Centers

A carbon with 2 identical groups is NOT chiral!

💡

Pro Tip: Fischer Projections

Vertical lines go back, horizontal lines come forward. Makes R/S easier!